Sinteza in karakterizacija novih fosfazenov Synthesis and characterisation of the new phosphazenes /
V prispevku so navedene in opisane strukture novih fosfazenov ter podane njihove sinteze. Spojine smo pripravili v argonovi atmosferi z reakcijami metilsulfonamida in dimetilsulfamida s PCl5 in (C6H5)3PCl2 v različnih topilih. Trdne produkte smo izločili z izparevanjem topila takoj po reakcijah.Te,...
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| Main Authors: | , |
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| Format: | Software Book Chapter |
| Jezik: | Slovenian |
| Teme: | |
| Sorodne knjige/članki: | Vsebovano v:
Slovenski kemijski dnevi 2010, Maribor, 23. in 24. september 2010 |
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| LEADER | 01935naa a2200289 ib4500 | ||
|---|---|---|---|
| 001 | 14436374 | ||
| 003 | SI-MaCOB | ||
| 005 | 20120315000000.0 | ||
| 006 | m|||||q||d|||||||| | ||
| 007 | co|||| | ||
| 008 | 101006s2010 xv |||||q|||||||| ||slv c | ||
| 041 | 0 | |a slv |b slv |b eng | |
| 080 | |a 66 | ||
| 100 | 1 | |a Dojer, Brina. |4 aut | |
| 245 | 0 | 0 | |a Sinteza in karakterizacija novih fosfazenov |h [Elektronski vir] = |b Synthesis and characterisation of the new phosphazenes / |c Brina Dojer, Ferdinand Belaj. |
| 246 | 3 | 1 | |a Synthesis and characterisation of the new phosphazenes |
| 300 | |a 9 str. | ||
| 504 | |a Bibliografija: str. 6. | ||
| 504 | |a Povzetek ; Abstract. | ||
| 520 | |a V prispevku so navedene in opisane strukture novih fosfazenov ter podane njihove sinteze. Spojine smo pripravili v argonovi atmosferi z reakcijami metilsulfonamida in dimetilsulfamida s PCl5 in (C6H5)3PCl2 v različnih topilih. Trdne produkte smo izločili z izparevanjem topila takoj po reakcijah.Te, na zraku nestabilne spojine, smo karakterizirali z monokristalno analizo pri 100 K. | ||
| 520 | |a Reactions of methylsulfonamide and dimethylsulfamide with PCl5 and (C6H5)3PCl2in different solvents have been studied. During our work we have synthesized 4 new and one, already known, fosfazene compounds. We characterised them only with single crystal X-ray structure analysis because of their nature of decomposing on air. Some of these compounds have already been synthesized in 1950s and 1960s, but their crystal parameters coud not be found in the literature. | ||
| 653 | 0 | |a fosfazeni |a sinteza |a karakterizacija | |
| 700 | 1 | 2 | |a Belaj, Ferdinand. |4 aut |
| 773 | 0 | |a Slovenski kemijski dnevi (2010 : Maribor) |t Slovenski kemijski dnevi 2010, Maribor, 23. in 24. september 2010 |d [Maribor] : FKKT, [2010] |w 8452937 |z 9789612482404 |g 9 str. | |
| 040 | |a KTFMB |b slv |c SI-MaIIZ |d KTFMB |e ppiak | ||
| 040 | |a KTFMB |b slv |c SI-MaIIZ |d KTFMB |e ppiak | ||
| 040 | |a KTFMB |b slv |c SI-MaIIZ |e ppiak | ||